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This is a known consideration in freeze-dried and frozen formulation research, where excipients such as mannitol are studied specifically to protect molecules through these phase changes, as covered in the Journal of Pharmaceutical Sciences review cited above

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2 Although MPH also inhibits the reuptake of norepinephrine, the literature supports the notion that the primary mechanism of clinical improvement of cognition is through its modulation of dopamine levels

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For researchers running microdose protocols or titrating doses in very small increments, this level of precision is valuable