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Conflict of interest All authors certify that they have no affiliations with or involvement in any organization or entity with any financial interest (such as honoraria

Untargeted metabolomics was performed by injecting 3 L of each sample onto a 10 cm C18 column (Thermo Fisher, CA) coupled to a Vanquish UHPLC running at 0.3mL/min using water and 0.1% formic acid as solvent A and acetonitrile and 0.1% formic acid as solvent B

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