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Analytical equipment VOC in e -liquids Clarus SQ 8 Gas Chromatograph/Mass Spectrometer (Perkin Elmer Inc.) VOC in aerosol Clarus SQ 8 Gas Chromatograph/Mass Spectrometer (Perkin Elmer Inc.) Column (liquid sample) Elite -VMS (30 m, 0.25 mm ID, 1.4 m) (Perkin Elmer Inc.) Column (aerosol sample) Elite -VRX (30 m, 0.25 mm ID, 1.4 m) (Perkin Elmer Inc.) Injection mode Split 10:1 Injection temperature Injection volume 250C 1.0 L Carrier gas Helium (purity 99.999%), constant flow Flow rate 2.0 mL/min Oven 35C was held for 1 minute then ramped at rate of 11C/minute to 190C, and then ramped at rate 15C/minute of which was further held for 3 minutes Source temperature 220C Interface temperature Run time 250C 20 min Acquisition mode Scan range Full scan mode m/z 15 - 400, library search against the NIST 11 mass spectral database Data processing Turbo Mass Software version 6.1.0 were identified from their resultant aerosol samples

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