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10.1186/1743-7075-10-44 [PMC free article: PMC3727955] [PubMed: 23783067] [CrossRef] Collison KS, Makhoul NJ, Zaidi MZ, Saleh SM, Andres B, Inglis A, et al

The first step is to react commercially available IR-780 iodide with excess anhydrous piperazine in anhydrous N , N -dimethyl formamide at 85 C to form cyanine-piperazine (CP)